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dc.contributor.authorTaskin, Omer S.
dc.contributor.authorBalkis (Caglar), Nuray
dc.contributor.authorAksu, Abdullah
dc.contributor.authorKorkmaz, Nagihan
dc.contributor.authorCetintasoglu, Mehmet Emre
dc.contributor.authorTorlak, Cihan
dc.date.accessioned2021-03-05T13:26:57Z
dc.date.available2021-03-05T13:26:57Z
dc.date.issued2018
dc.identifier.citationTaskin O. S. , Aksu A., Cetintasoglu M. E. , Korkmaz N., Torlak C., Balkis (Caglar) N., "Preparation of analytical columns and HPLC silica-based C-18 packing material synthesis from non-toxic silica source", JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, cilt.41, ss.583-587, 2018
dc.identifier.issn1082-6076
dc.identifier.othervv_1032021
dc.identifier.otherav_b23c2db4-5728-4e6b-b963-562be8a0edeb
dc.identifier.urihttp://hdl.handle.net/20.500.12627/118739
dc.identifier.urihttps://doi.org/10.1080/10826076.2018.1469511
dc.description.abstractStudies about stabilization and lowering the activity of the permanent groups of stationary phases that are used in reversed-phase liquid chromatography (RP-HPLC) considerably increased during the last few decades. In gas and liquid chromatography, silica gels are generally used for as a solid support due to their low price and various particle size products. Moreover, they have a good mechanical stability and swelling resistance. It also provides high efficiency and has different pore sizes that make it easy to make changes in different shapes. In this study, sol-gel is used to synthesis silica gels and during gelation process surfactants are added to attain spherical morphology. Conventional silica gel precursors are predominantly silicone alkoxides with high purity but they are also highly hazardous materials. Therefore, water glass is used as a precursor in our study and C-18 groups are linked to silica gels. For C-18 linking process, trimethoxyocta decyl silane and trichloroocta decyl silane are tested individually as a cross-linking agent and their performances are compared with various analyses.
dc.language.isoeng
dc.subjectTıp
dc.subjectKimya
dc.subjectMoleküler Biyoloji ve Genetik
dc.subjectSağlık Bilimleri
dc.subjectTemel Tıp Bilimleri
dc.subjectBiyokimya
dc.subjectYaşam Bilimleri
dc.subjectMoleküler Biyoloji ve Genetik
dc.subjectSitogenetik
dc.subjectAnalitik Kimya
dc.subjectTemel Bilimler
dc.subjectBİYOKİMYASAL ARAŞTIRMA YÖNTEMLERİ
dc.subjectBiyoloji ve Biyokimya
dc.subjectYaşam Bilimleri (LIFE)
dc.subjectKİMYA, ANALİTİK
dc.subjectTemel Bilimler (SCI)
dc.subjectBİYOKİMYA VE MOLEKÜLER BİYOLOJİ
dc.titlePreparation of analytical columns and HPLC silica-based C-18 packing material synthesis from non-toxic silica source
dc.typeMakale
dc.relation.journalJOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES
dc.contributor.departmentKırklareli Üniversitesi , ,
dc.identifier.volume41
dc.identifier.issue10
dc.identifier.startpage583
dc.identifier.endpage587
dc.contributor.firstauthorID104340


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